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XAFS

XAFS2300 X-ray Absorption Fine Structure Spectrometer

X-ray absorption fine structure spectrometer is a supplement and extension of synchrotron radiation, and does not rely on synchrotron radiation laboratory level XAFS and XES measurement devices.It is a laboratory level XAFS and XES measurement instrument that does not rely on synchrotron radiation light sources.

Our XAFS2300 integrates three core components: a high-throughput continuous spectrum X-ray source, a high reflection efficiency curved crystal monochromator, and a high-resolution SDD detector. It can achieve precise measurement XAFS in laboratory environment, and complete the analysis of coordination number, bond length, chemical valence state, and coordination configuration of elements.In addition, XAFS2300 can also perform XES testing, which is essentially an ultra-high energy resolution X-ray fluorescence spectrum, achieving accurate determination of element spin-state and neutron like near coordination element species.

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 Comparison of XAFS and synchrotron radiation data



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Cu foilcrystal structure

Parameters

Power: 3kW

luminous flux: >2×106 photons/sec. (7-9keV), equipped with transmission mode and fluorescence mode X-ray absorption fine structure spectroscopy (XAFS) and X-ray emission spectroscopy (XES) measurement functions

Energy Range: 4.5-25keV

Energy Resolution: 0.5-3eV

Repeatability:< 50meV, energy scale drift, monochromator does not require repeated calibration 

Adopting a high-resolution Roland ring structure and a spherical curved X-ray monochromator; High resolution SDD detector. Able to complete 1% actual sample measurement.


Application

XAFS has become an important characterization tool for studying the local atomic and electronic structures of materials in the fields of materials science and engineering. Widely used in the research of nanomaterials, semiconductor materials, chemical catalytic materials, biomaterials, mineral analysis, military materials, etc., it is an essential method in the cutting-edge research field of condensed matter physics in the future.

Catalysis: multiphase catalysis, single atom catalysis, etc.; the relationship between catalyst atoms and carriers;

Energy: battery materials, fuel cell catalysts, photosynthesis, carbon capture, hydrogen production

Materials: doping, ion migration, valence state, structural crystal form;

Environment: valence states of toxic elements and their circulation in nature; The chemical state of radioactive isotopes;

Biology: Plant absorption/cycling of metal proteins and metal elements.


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Application of XAFS in Accurate Material Structure Analysis of Carbon Neutrality and Efficient CO2 Conversion Energy Catalysis Materials


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XAFS fluorescence mode implementation for testing 1% low content single atom catalyst system


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1% Cu CuN4-C Single atom catalyst